簡介
ProboStat ACIS System
ProboStat™ ACIS 是一種樣品支架,專門用於在高溫和受控氣氛下對小圓盤樣品進行交流電導率測量和雙電極阻抗阻抗分析。
與標準 ProboStat™ 裝備相比,熱區零件的特殊設計方便安裝和更換測試樣本。
ProboStat™ ACIS 是一種樣品支架,專門用於在高溫和受控氣氛下對小圓盤樣品進行交流電導率測量和雙電極阻抗阻抗分析。
與標準 ProboStat™ 裝備相比,熱區零件的特殊設計方便安裝和更換測試樣本。
測試樣品放置在支撐管中,與電極接觸,並由彈簧負載組件穩固固定。此裝置以單腔模式組裝,幾乎可輸入任何氣體。樣品架的設計可在接近大氣壓力下操作,但也可抽至低真空,或保持高達 15 bar 的壓力。
透過標準同軸電纜進行電氣連接。
ProboStat™ ACIS 兼容性
本系統隨附標準 ProboStat™ 基本裝置,並可擴充 ProboStat™ 可支援的任何樣品幾何形狀與量測。
ProboStat™ ACIS 可與所有儀器搭配使用,例如Novocontrol、Gamry等廠牌的阻抗分析儀、LCR 計和恒電位儀。
ProboStat™ ACIS System 設定:
ProboStat™ ACIS 規格
溫度範圍:
•RT - 1600 °C。
氣氛:
•氧化、惰性、還原。
•濕、乾。
•腐蝕性 ( 可選 )。
•0.01 mbar - 1 bar(可選 15 bar)。
基座裝置
•6 個 BNC 電極連接。
•3 個熱電偶接頭。
•4 個世偉洛克Swagelok快速接頭 - 兩個氣體輸入和兩個氣體輸出。
•16 個迷你接點,用於可拆式電極接點和熱電偶。
•3 個開關,用於接地和屏蔽選項。
•冷卻/加熱水軟管配件。
熱區零件
•特殊設計的氧化鋁樣品支撐管。
•氧化鋁彈簧負載組件。
•2 個電極接點 鉑金+氧化鋁。
•熱電偶:S 或 K 型。
測試樣品尺寸:
•圓盤直徑:最大 15 mm。
•高度:最大 10 mm。
外部系統尺寸:
•包圍管直徑:40 mm。
•總長度: 75 cm。
測量的材料特性和適用的方法:
•交流電導率 vs T、pO2, pH2O 等。
•阻抗分析。
•晶體、晶界和電極阻抗。
•H/D 同位素效應。
•燃料電池元件測試。
•介電特性。
ProboStat™ ACIS is a sample holder dedicated for AC conductivity measurements and 2-electrode impedance spectroscopy on small disk samples at high temperatures and under controlled atmospheres.
Special design of the hot-zone parts facilitates mounting and replacement of test samples compared with the standard ProboStat™ furnishment.
The test sample rests in a support tube, is contacted by electrode connects, and held stably in place with a spring load assembly. The setup is assembled in a single chamber mode and can be fed with virtually any gas. The sample holder is designed to operate at near-atmospheric pressure, but can be pumped to low vacuum, or hold up to 15 bar. Electrical connections are made via standard coax cables.
ProboStat™ ACIS Compatibility
The system is supplied with a standard ProboStat™ base unit and can be expanded for any sample geometries and measurements that ProboStat™ can support.
The ProboStat™ ACIS works well with all instrumentation such as impedance spectrometers, LCR meters and potentiostats from Solartron, PAR, Novocontrol, Autolab, Gamry, HP/Agilent, etc.
Fig. ProboStat™ ACIS setup:
ProboStat™ ACIS Specifications
Temperature range:
•RT - 1600 °C
Atmospheres:
•Oxidizing, inert, reducing
•Wet, dry
•Corrosive optional
•0.01 mbar - 1 bar (15 bar optional)
Base unit:
•6 BNC electrode connections
•3 thermocouple connections
•4 Swagelok quick-connects - two gas in and two gas out
•16 mini-contacts for detachable electrode contacts and thermocouples
•3 switches for grounding and shielding options
•Cooling/heating water hose fittings
Hot zone parts:
•Specially designed sample support tube of alumina
•Spring-load assembly of alumina
•2 electrode contacts: Pt+alumina
•Thermocouple: type S or K
Test sample size:
•Disk diameter: max 15 mm
•Height: max 10 mm
Outer system dimentions:
•Enclosing tube diameter: 40 mm
•Overall length: 75 cm
Materials properties measured and applicable methods:
•AC conductivity vs T, pO2, pH2O, etc.
•Impedance spectroscopy
•Bulk, grain boundary and electrode impedance
•H/D isotope effect
•Fuel cell components test
•Dielectric propertie