產品介紹∣PEM /AEM水電解測試槽 NREL 高壓低溫電解( LTE) 槽
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PEM /AEM水電解測試槽 NREL 高壓低溫電解( LTE) 槽
NREL High-Pressure Low-Temperature Electrolysis Cell

【Redox.me】電化學周邊耗材 電化學流動系統

PEM /AEM水電解測試槽  NREL 高壓低溫電解( LTE) 槽

簡介

NREL High-Pressure Low-Temperature Electrolysis Cell

由美國國家可再生能源實驗室 (NREL) 開發的高壓低溫電解 (LTE) 槽是在呈現開放式的硬體設計,可讓所有使用者自由修改與重複性組裝。
這項工作由美國能源部的 H2NEW 聯盟規劃並資助。

我要諮詢

由美國國家可再生能源實驗室 (NREL) 開發的高壓低溫電解 (LTE) 槽是在呈現開放式的硬體設計,可讓所有使用者自由修改與重複性組裝。
這項工作由美國能源部的 H2NEW 聯盟規劃並資助。

Redox.me提供根據NREL 技術文件製作的 25 cm² PEM 變異,以及redox.me根據NREL指南開發的其它變異形式。在前者中,流場模式直接轉換自 25 cm² PEM 變體。
這些產品的傳播目的在於方便廣大使用者輕鬆使用此設備。然而,如果您有能力自行生產 25 cm² PEM 變異,我們鼓勵您使用已是開放的原始設計圖去更改成新的設計。
如果您有自己的技術資源,這可能是一個更具成本效益的選擇。我們提供25 cm² PEM 變體的 3D CAD 模型和 2D 技術圖紙參考。

高壓 LTE 運行可以降低運營成本,因為與使用下游機械壓縮機相比,生產電化學加壓氫氣的效率更高。同時,該單元也與常壓(環境壓力) LTE 相容。

該單元可以容納不同厚度的多孔傳輸層。為了實現這一點,可以增加單元每側的墊片數量,從而為多孔傳輸層提供更大的體積。

在較小的表面積型號(1 cm² 和 4 cm²),有一個優點是它們與電化學工作站和增幅器的測試相容性。在這些情況下,需求的電流數通常在大多數增幅器可接受的範圍內。
然而,對於電流密度高達 6 A/cm² 的較大活性表面,可能需要高功率可程式直流電源供應器。

應用說明
以下連結的文件和圖紙概述了低溫電解硬體的設計,旨在滿足 ASME B31.1 的洩漏測試標準。這些文件和圖紙也提供了全面的電池組裝說明和性能基準測試程序。
在環境壓力和高壓力下安全操作的責任完全在於最終使用者,且每個電池都應根據個別情況進行評估。密封效果可能會受到加工品質、元件組裝、操作條件和操作歷史等因素的影響。
壓力操作只能在合格的測試台上由訓練有素的操作人員進行。
*Wrubel, Jacob, Samantha Ware, Corey Schaffer, Matt Allen, Ellis Klein, Robin Rice, Chaiwat Engtrakul, and Guido Bender. 2023. 
"NREL 25-cm2 High-Pressure Low-Temperature Electrolysis Cell Hardware (Open Source).
" NREL Data Catalog. Golden, CO: National Renewable Energy Laboratory. https://doi.org/10.7799/2205626 
  


  
 

 

Cell
active area: 25 cm², 4 cm² or 1 cm² (other on request)
maximum verified working pressure: 30 bar
flow field design: triple serpentine (other on request)
temperature sensor
sensor type: Pt100 x2 (100  at 0 ºC)
construction: Wire-Wound, 10 mm tails
fundamental interval: 38.5  (nominal)
self-heating: 0.02 to 0.3 ºC/mW
thermal response: <0.4 s
measuring current: 1 mA
diameter: 1.5 mm
length: 15 mm
tolerance class (IEC 60751): Class A
temperature range: -200 ºC to +650 ºC
body material: alumina
adhesive-backed pad heater
power source: electric
voltage: max 60 V
power: max 59 W
resistance: 61 Ω
material: polyimide
maximum temperature: 250 ºC
wire type: silicone braided wire
insulating resistance: >5 MΩ
size: 50 mm x 50 mm
thickness: <0.266 mm
adhesive: 3M
wire length: 60 mm
fittings
body material: Stainless Steel 316
connection 1 size: 1/4 in. tube OD (6.35 mm)
connection 1 type: Swagelok® Tube Fitting
connection 2 size: 7/16-20 in.
connection 2 type: male SAE/MS straight thread
reference: Swagelok® part #: SS-400-5-4ST
List of Materials
anode flow field (PEM): platinum coated titanium (grade II)
cathode flow field (PEM): gold coated titanium (grade II)
anode flow field (AEM): pure nickel
cathode flow field (AEM): pure nickel
threaded end plate: anodized aluminium 
unthreaded end plate: anodized aluminium
current collectors: gold coated (nickel interlayer) copper (101)
fittings: Stainless Steel 316
bolts: zinc yellow-chromate plated steel grade 8
gaskets: skived PTFE and FKM
washers: Stainless Steel18/8
Belleville washers: Stainless Steel 302
insulating tape: PEEK
alignment pins: PFA
temperature sensor body: alumina
adhesive backed pad heater: polyimide with 3M adhesive
Setup includes
1 x anode flow field
1 x cathode flow field
1 x threaded end plate 
1 x unthreaded end plate 
2 x current collector
4 x Swagelok® part #: SS-400-5-4ST fitting
8 x bolt
10 x FKM gasket
10 x skived PTFE gasket 
16 x washer
64 x Belleville washer
2 x insulating PEEK tape
4 x alignment pin 11 mm long, 3 mm OD
2 x alignment pin 8 mm long, 3 mm OD
2 x dual Pt100 temperature sensor
2 x adhesive backed pad heater

 

Developed by National Renewable Energy Laboratory (NREL) High-Pressure Low-Temperature Electrolysis (LTE) Cell is on open-source cell hardware designed for repeated reassembly. This work was planned and funded by the U.S. Department of Energy’s H2NEW consortium.

Redox.me offers a 25 cm² PEM variant produced based on the technical documentation from NREL, as well as other variants developed by redox.me according to NREL guidelines. In the former, the flow field pattern is directly translated from 25 cm² PEM variant. The dissemination of these products aims to facilitate easy access to this equipment for a wide range of users. However, if you have the capability to produce the 25 cm² PEM variant on your own, we encourage you to use the open-source files. It may turn out that if you have access to your own technical resources, this will be a more cost-effective option. 3D CAD models and 2D technical drawings for variant 25 cm² PEM are available for download. 

High pressure LTE operation can reduce operating costs, as it is more efficient to produce electrochemically pressurized hydrogen compared to using downstream mechanical compressors. However, the cell is also compatible with ambient pressure LTE.
The cell can accommodate porous transport layers of varying thicknesses. To achieve this, the number of gaskets on each side of the cell can be increased, providing a larger volume for the porous transport layer.
One benefit of the smaller surface area variants (1 cm² and 4 cm²) is their compatibility for testing with a potentiostat and booster. In these cases, the current levels are typically within the acceptable range for most boosters. However, for larger active surfaces with current densities up to 6 A/cm², a high-power programmable DC power supply may be required.

Application note
The documents and drawings linked below outline the design of low-temperature electrolysis hardware that is intended to meet leak testing standards as per ASME B31.1. They also provide comprehensive cell assembly instructions and a procedure for performance benchmarking. The responsibility for safe operation at both ambient and elevated pressures lies solely with the end user, and each individual cell should be assessed on a case-by-case basis. The sealing effectiveness may be influenced by factors such as machining quality, components used in cell assembly, operating conditions, and the operational history. Pressure operations should only be conducted on qualified test stands by trained operators.
Wrubel, Jacob, Samantha Ware, Corey Schaffer, Matt Allen, Ellis Klein, Robin Rice, Chaiwat Engtrakul, and Guido Bender. 2023. "NREL 25-cm2 High-Pressure Low-Temperature Electrolysis Cell Hardware (Open Source)." NREL Data Catalog. Golden, CO: National Renewable Energy Laboratory. https://doi.org/10.7799/2205626 
  

  

 

Cell
active area: 25 cm², 4 cm² or 1 cm² (other on request)
maximum verified working pressure: 30 bar
flow field design: triple serpentine (other on request)
temperature sensor
sensor type: Pt100 x2 (100  at 0 ºC)
construction: Wire-Wound, 10 mm tails
fundamental interval: 38.5  (nominal)
self-heating: 0.02 to 0.3 ºC/mW
thermal response: <0.4 s
measuring current: 1 mA
diameter: 1.5 mm
length: 15 mm
tolerance class (IEC 60751): Class A
temperature range: -200 ºC to +650 ºC
body material: alumina
adhesive-backed pad heater
power source: electric
voltage: max 60 V
power: max 59 W
resistance: 61 Ω
material: polyimide
maximum temperature: 250 ºC
wire type: silicone braided wire
insulating resistance: >5 MΩ
size: 50 mm x 50 mm
thickness: <0.266 mm
adhesive: 3M
wire length: 60 mm
fittings
body material: Stainless Steel 316
connection 1 size: 1/4 in. tube OD (6.35 mm)
connection 1 type: Swagelok® Tube Fitting
connection 2 size: 7/16-20 in.
connection 2 type: male SAE/MS straight thread
reference: Swagelok® part #: SS-400-5-4ST
List of Materials
anode flow field (PEM): platinum coated titanium (grade II)
cathode flow field (PEM): gold coated titanium (grade II)
anode flow field (AEM): pure nickel
cathode flow field (AEM): pure nickel
threaded end plate: anodized aluminium 
unthreaded end plate: anodized aluminium
current collectors: gold coated (nickel interlayer) copper (101)
fittings: Stainless Steel 316
bolts: zinc yellow-chromate plated steel grade 8
gaskets: skived PTFE and FKM
washers: Stainless Steel18/8
Belleville washers: Stainless Steel 302
insulating tape: PEEK
alignment pins: PFA
temperature sensor body: alumina
adhesive backed pad heater: polyimide with 3M adhesive
Setup includes
1 x anode flow field
1 x cathode flow field
1 x threaded end plate 
1 x unthreaded end plate 
2 x current collector
4 x Swagelok® part #: SS-400-5-4ST fitting
8 x bolt
10 x FKM gasket
10 x skived PTFE gasket 
16 x washer
64 x Belleville washer
2 x insulating PEEK tape
4 x alignment pin 11 mm long, 3 mm OD
2 x alignment pin 8 mm long, 3 mm OD
2 x dual Pt100 temperature sensor
2 x adhesive backed pad heater