產品介紹∣高溫材料測試爐|樣本座

Solartron Analytical - 精密阻抗測試設備設計專家，與高溫爐專業廠家Carbolite及樣本座專業廠家NorECS攜手協力，合作生產一系列先進的高溫材料特性測試系統。
材料特性測試的靈活解決方案：
- 系統採用一個開合式的管型爐設計及一個升降台，可以輕鬆的取放樣本及進行定位。
- 樣本是放置在鉑電極之間一個專門設計的樣本座內，可在極高溫下接受測試。
- 進行固體氧化物應用測試時，也可在樣本的任一邊施放氣體。
- 應用包括：
  - 固態、固體氧化物、超離子、電子陶瓷材料的開發。
  - 儲能應用包括SOFC固態氧化物燃料電池及固態電池。
  - 航空航天/汽車應用：高溫絶緣礙子、制動器、渦輪葉片。
高性能溫度控制系統：結合129620A高溫爐及129621A/B/C樣本座，可產生高性能的溫度控制系統，具備全方位的測試性能：
- 使用一個精密Eurotherm 2000系列溫度控制器，操作範圍從室溫到1,200 ºC。
- 提供因應材料需求的各種樣本座結構配置：2端/4端/van der Pauw 4點量測法。
- 雙重燃氣供應：適用於SOFC類型應用。
- 控制的大氣組成。
- 適用於各類型樣本、盤型、條狀..等。
完整的材料測試系統：
- 129620A高溫爐及129621A/B/C樣本座選購，可搭配Solartron各型材料測試系統，以進行I-V、脈衝、C-V、阻抗、Mott-Schottky及其它廣泛的材料測試法，完全與溫度控制整合。
- 個人電腦軟體，提供完全整合的電氣測量與溫度控制功能。
- 高/低阻抗材料，可依選擇的儀器及樣本座結構，而進行分析。
- 提供樣本測量與參考及標準化測量方式的比較，以提高測量精度。
- 寬廣的頻率範圍：從µHz～＞MHz。
- 寬廣的阻抗測量範圍～＞TΩ。

129620A高溫爐：
- 高溫爐：客製的Carbolite VST12/300。
- 高溫爐類型：垂直開合式帶鉸鏈的管型爐設計，可輕易取放樣本座。
- 溫度範圍：室溫～1,200°C（*其它溫度範圍，請洽詢）。
- 溫度穩定性：＜1°C。
- 溫度解析度：0.1°C。
- 加熱元件：嵌在真空成型陶瓷纖維半圓柱體內的螺旋線圈。
- 結構：
  - 嵌在陶瓷纖維中的加熱元件，連同纖維板與纖維棉毯，構成絶緣體的一部分。
  - 外殼：帶網孔的不鏽鋼罩，給予操作人員最高程度的安全性。
- 加熱長度：300 mm。
- 實體設置：
  - 使用一個桌上立架將高溫爐定位在550、650或750 mm處（從底座到加熱區中間）。
  - ProboStat樣本座高度，可使用升降台調整（80 mm）。
- 控制熱電耦：可選擇內部爐子或ProboStat熱電耦。
- 主控制器：Eurotherm 2416CG經ModBus RS232介面，連接到個人電腦。
- 過溫偵測/關機：內部爐子礦物絶緣式N型熱電耦，直接連接到由Eurotherm 2132溫度控制器控制的過溫安全保護系統。
129621A/B/C樣本座：
- 高溫樣本座：NorECS ProboStat™底座黃銅（-A/B/C）或不鏽鋼（-SA/SB/SC）。
- 加熱區部件：
  - 裝有彈簧的樣本支撐管 - 氧化鋁。
  - 燃氣供應管 - 氧化鋁/矽石。
  - 電極連接 - 鉑及氧化鋁。
  - 熱電偶，S型。
- 樣本類型：
  - 129621A：只限盤型（一般型）。
  - 129621B：盤型及條狀（進階型 - 適用範圍更廣）。
  - 129621C：只限盤型（簡單型）。
- 樣本盤尺寸：
  - 建議樣本直徑20 mm（可要求10～24 mm直徑）。
  - 最大直徑15 mm（129621C）。
- 條狀樣本最大尺寸：長25～50 mm。
- 溫度範圍：室溫～1,200°C，依高溫爐規格而定。
- 溫度精度：典型為1°C，依熱電耦使用壽命、校正及使用者專業程度而定。
詳細規格、配件、軟體及選購，歡迎洽詢。

Solartron Analytical, specialists in the design of precision impedance test equipment, has joined forces with high temperature Furnace specialists Carbolite, and sample holder specialists NorECS to produce a range of advanced high temperature materials characterization test systems.
The flexible solution for materials characterization...
- The system uses a split tube furnace design together with a lab jack that allows easy sample access and positioning. The sample is positioned in a purpose designed sample holder between platinum electrodes that allow testing at very high temperature. Gases may also be applied to either side of the sample for solid oxide applications.
- Applications include:
  - Development of solid state, solid oxide, superionic, electro-ceramic materials
  - Energy applications include SOFC fuel cell and solid state battery
  - Aerospace/automotive applications – high temperature insulators, brakes, turbine blades
High Performance Temperature Control:
- The 129620A furnace with 129621A/B/C sample holders combine to produce a high performance temperature control system with comprehensive test facilities:
- Operating range room temperature to 1200ºC using a precise Eurotherm 2000 series temperature controller.
- Various sample holder configurations are available depending on material requirements – 2 terminal/4 terminal/van der Pauw
- Dual gas supply is available for SOFC type applications
- Controlled atmospheres.
- Various sample types can be accommodated, disk, bar etc.
Complete Materials Test Systems:
- The 129620A high temperature furnace with 129621A/B/C sample holder options may be used together with various Solartron materials test systems to run I-V, Pulse, C-V, Impedance, Mott-Schottky and a wide range of other materials test techniques, fully integrated with temperature control.
- PC software provides fully integrated electrical measurements with temperature control.
- High and low impedance materials can be analyzed depending on the choice of instrumentation and sample holder configuration
- Sample vs. reference and normalization techniques are provided for improved measurement accuracy.
- Wide frequency range from µHz to > MHz
- Wide impedance range to > Tohms

129620A High Temperature Furnace Specification
- High Temperature Furnace: Customized Carbolite VST12/300
- Furnace type: Vertical, hinged, split tube furnace for easy access to sample holder
- Temperature range: Room temperature to 1200°C (Contact us for other temperature ranges)
- Temperature stability: Stability: < 1°C
- Temperature resolution: 0.1°C
- Heating elements: Spiral wire coils embedded in vacuum formed ceramic fibre half cylinders
- Construction:
  - Heating elements embedded in ceramic fibre forms part of insulation together with fibre board and blanket.
  - Outer case stainless steel with mesh cover for maximum operator safety
- Heated length: 300 mm
- Physical setup:
  - Furnace is positioned 550, 650 or 750 mm (from base to middle of heated zone) using a desk top stand.
  - ProboStat sample holder height is adjustable (80 mm) using 'Lab-Jack'
- Control thermocouple: Selectable between internal furnace and ProboStat thermocouple
- Main Controller: Eurotherm 2416CG connected to PC via ModBus RS232 interface
- Overtemperature detection/shutdown: Internal furnace mineral insulated Type N thermocouple hard-wired to over-temperature safeguard controlled by a Eurotherm 2132 temperature controller
129621A/B/C Sample Holder Specifications:
- High Temperature Sample Holder: NorECS ProboStat™ base unit brass (-A/B/C) or stainless steel (-SA/SB/SC)
- Hot zone parts:
  - Spring-loaded sample support tubes, alumina;
  - as supply tubes, alumina / silica;
  - Electrode connects, Pt and alumina
  - Thermocouples, S type
- Sample types:
  - 129621A - disk only (normal)
  - 129621B - disk & bar (extensive)
  - 129621C - disk only (easy load)
- Sample disk size:
  - 20 mm sample diameter recommended (10-24 mm diameter upon request)
  - Max diameter 15 mm for ‘129621C’
- Max. size bar sample: 25-50 mm long
- Temperature range: Room Temperature to 1200°C depending on range of furnace
- Temperature accuracy: Typically 1°C, depending on thermocouple life, calibration, and user expertise
Please feel free to contact for detailed specifications, accessories, software and options.