產品介紹∣ISS COMPACT VIS - INTEGRATED SPECTROCHEMICAL SYSTEM COMPACT VIS
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ISS COMPACT VIS - INTEGRATED SPECTROCHEMICAL SYSTEM COMPACT VIS

【Redox.me】電化學周邊耗材 實驗室儀器

ISS COMPACT VIS - INTEGRATED SPECTROCHEMICAL SYSTEM COMPACT VIS

簡介

INS-ISS_COMPACT_VIS

The Compact Line of integrated spectrochemical instruments is targeted at proof of concept and early-stage research and educational purposes.

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Compact 系列集成光譜化學儀器旨在驗證概念以及早期研究和教育目的。每個 compact line 儀器包括:Avantes Compact Line 光譜儀、Avantes 光源、蠕動泵、專用光譜電化學池(帶柱的比色杯)的支架和固定在 30 cm x 45 cm 固體鋁光學板上的電解質儲液器。選擇組件並優化設計以確保在實驗室通風櫥下操作時佔地面積小、易於使用、良好的分析性能和安全性。

該系統的核心是從各種 redox.me 產品(單獨添加)中選擇的光纖耦合光譜電化學電池。通過使用端接在准直透鏡中的光纖,可以實現簡單的組裝和可重複的對準。

電解質通過蠕動泵從儲液器輸送到電池。泵頭有 1 個通道,通過矽膠或 Viton™/Fluran™ F-5500-A(水性電解質)或 PharMed™(有機電解質)內管以每分鐘 0.07 至 380 毫升的流速泵送電解質,並且FEP 管進一步連接到電池/儲液器。 

通過光纖耦合的 Avantes Compact Line 光譜儀和光源進行光譜分析。提供 UV、Vis、NIR、寬範圍 UV-Vis 和雙通道“超寬”UV-VIS-NIR 區域的預配置集成系統。這些預配置系統與光源、光纖、透鏡和光譜儀配置相匹配,可在指定的光譜範圍和分析應用中提供優化的性能,但可以額外付費配置定制系統以滿足嚴格的最終使用要求。有關定制光譜儀和儀器配置的更多信息,請聯繫 redox.me。

集成系統中使用的所有光源都配備了 TTL 快門或觸發器,以將樣品的光照減少到絕對最低限度。源由與光譜儀相同的軟件觸發,允許以用戶定義的參數和間隔進行簡單的實驗設計和同步測量。通過使用 TTL 快門和/或脈衝光源,可以最大限度地減少不良熱效應並確保穩定的光源以最大限度地減少漂移。

選擇光纖以最小化光譜吸收並優化光源和光譜儀的耦合,從而在不使光譜儀飽和的情況下最大化輸送到細胞的可用光。這允許更快的積分時間和增加的信號平均,以提高測量的信噪比。

The Compact Line systems are supplied with Avasoft Full version 8.11 plus the chemometrics extension for simple data acquisition and post processing as well as process monitoring and real-time calculation of analyte concentration. Additional Avantes software modules such as Thin Film analysis and colourimetry are available for other applications at an additional cost.

Application note
The Integrated Spectrochemical System Compact Vis (ISS Compact Vis) includes a AvaSpec-Mini2048CL-V25 spectrometer and an AvaLight-HAL-S-Mini tungsten halogen lamp coupled to the spectro-electrochemical flow cell by Low OH SMA 905 terminated optical fibres. This system is suitable for visible light transmission spectroscopy with good resolution and sensitivity.

The following cells are compatible with ISS Compact Vis (please select desired option and add it to the quotation separately):

  • Cell 1: SPECTRO-EFC, SMA 905, 1.75 mL
  • Cell 2: SPECTRO-EFC, 4 mm path, 0.7 mL, SMA 905 variant
  • Cell 3: R/T/A SPECTRO-EC, 1.75 mL, SMA 905 variant

The AvaLight-HAL-S-Mini is a compact stabilised Tungsten-Halogen light source equipped with a TTL-shutter and a filter slot that accepts 1 inch circular or 2 inch square filters to block specific wavelength ranges or attenuate the intensity of the source. The TTL-shutter allows for communication to the Avantes compact line spectrometer and auto-save dark reference in the AvaSoft spectroscopy Software.

The AvaSpec CompactLine spectrometers are compact and rugged spectrometers suitable for harsh environments. They deliver the resolution, sensitivity and stability that is expected from Avantes spectrometers in a form factor that is the size of a deck of cards. The AvaSpec-Mini2048CL-V25 delivers 0.7 nm resolution over the visible range between 350 – 850 nm. It is suitable for both spectrometric and colorimetric applications. If colourimetry is the main intended application then the Colour addon for AvaSoft is required, POI.

規格
光源:AvaLight-HAL-S-Mini
光譜輸出:360 – 2500 nm
穩定性:± 0.1%/ °C
穩定時間:ca。10 分鐘
燈泡輸出:12.0 VDC/0.83A
燈泡壽命:4000 小時
以上。光功率 200 µm 光纖:
最小 0.5 mWatt。光功率 600 µm 光纖:
最小4.5 毫瓦 光功率 1000 µm 光纖:10 mWatt
燈泡色溫:2,850 K
功率要求:12 VDC / 2.08A
連接器:SMA-905 連接器
尺寸,重量:150 x 78 x 37 毫米,510 克
快門壽命:1,000,000 次循環(典型)

Spectrometer: AvaSpec-Mini2048CL-V25
range: 350 – 850 nm
resolution: 0.7 nm
focal length: symmetrical Czerny-Turner, 75 mm focal length, MK II
grating: 600 lines/mm
entrance slit: 25 µm
dynamic range: 3300
signal/noise: 330:1
exposure time range: 30 µs to 40 s
stray light: 0.2 - 1%
sensitivity: 337,500
detector: HAM S11639 , CMOS linear array, 2048 pixels (14x200 μm)
A/D converter: 16-bit, 6 MHz
optical interface: SMA connector
I/O: 5 bidirectional programmable I/O; 1 analogue out; 1 analogue in, 1x5V
interface: USB 2.0 (480 Mbps) / pigtailed (40 cm) USB-A
dimensions, weight: 95 x 68 x 20 mm, 175 g

Light source to cell optical fibre
type: 0.39 NA pure silica core and TECS hard cladding, step-index, multimode fibre
termination: dual SMA 905,
coating : Tefzel
reinforcement: 5.0 mm stainless steel 
fibre: FT600EMT Low OH pure silica core for Visible-NIR
transmission: 400 - 2200 nm
length: 100 cm
core diameter: 600 ± 10 µm
numeric aperture: 0.39
cladding diameter: 630 ± 10 µm
coating diameter: 1040 ± 30 µm
bend radius short term/long term: 30 mm/60 mm

Cell to spectrometer optical fibre
type: 0.22 NA pure silica core and double-clad TECS hard cladding over fluoride-doped silica cladding, step-index multimode fibres
termination: dual SMA 905, 
coating : Tefzel
reinforcement: 5.0 mm stainless steel
fibre: FG200LCC Low OH pure silica core for UV – Visible Transmission 400 - 2200 nm
core diameter: 200 ± 8 µm
length: 100 cm
numeric aperture: 0.22
cladding diameter: 240 ± 5 µm
coating diameter: 260 ± 6 µm
bend radius short term/long term: 12 mm / 24 mm

Intrastat data
HS Code: 90273000
Country of Origin: Sweden
NET weight: 11000 g

產品包括
1 x 光譜儀 - AvaSpec-Mini2048CL-V25
1 x 光源 - AvaLight-HAL-S-Mini
1 x 光纖 - FT600EMT 低 OH 純矽膠芯
1 x 光纖 - FG200LCC 低 OH 純矽膠芯
1 x 蠕動泵,帶管道
1 x 儲液器 50 mL
1 x 鋁製麵包板,300 mm x 450 mm x 12.7 mm,帶橡膠腿和橋式手柄的 M6 絲錐
1 x PTFE 比色皿
1 x PTFE/PEEK 柱 1/4" 20 UNC 至 M6