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電池盒—三電極設置
BATTERY CARTRIDGE – THREE-ELECTRODE SETUP

【Redox.me】電化學周邊耗材 電池和超級電容器

電池盒—三電極設置

簡介

CTG-A-3ES-18

這是三電極電池測試單元和其它redox.me電池測試單元所附的標準電池盒。當研究人員想在三電極設置中對電池和超級電容器材料進行可重複的電化學量測時,它是理想的選擇。電池盒可以在電池基座之間交換。因此,若擁有多個電池盒,可在另一個電池盒處於清潔狀態時可使用另一個電池盒,讓您的實驗測試不會中斷。

我要諮詢

選擇電解液類型:

  • 有機電解質 
  • 水性電解質 

選擇電極直徑:

  • 18mm(標準)
  • 12mm
  • 15mm
  • 16mm

介紹
這是三電極電池測試單元和其它redox.me電池測試單元所附的標準電池盒。當研究人員想在三電極設置中對電池和超級電容器材料進行可重複的電化學量測時,它是理想的選擇。電池盒可以在電池基座之間交換。因此,若擁有多個電池盒,可在另一個電池盒處於清潔狀態時可使用另一個電池盒,讓您的實驗測試不會中斷。

  • 三電極裝置由上,下電極柱塞、隔板鎖環和參考電極沖頭組成。
  • 附的標準電極柱塞是為直徑為18 mm、總夾層厚度達2.5 mm的平面電極設計。
  • 隔板的直徑應至少比電極直徑大 2 mm(最大 22 mm)。鎖環將隔板固定在電極盒中,使電極的插入更加容易和安全,同時確保准確對準。
  • 上、下電極柱塞有多種材料可供選擇:316L 不銹鋼(標準)、銅、鋁、鎳等。
  • 針式參考電極從電極盒的側面安裝。由於針腳末端有尖銳的邊緣孔,參考電極(Li/Na/K等)可以很容易地從金屬箔上打孔下來,直接裝入電池。
  • 對於雙電極測量,可以使用參考電極沖頭封閉參考電極饋通孔。
  • 電池元件是用對樣品有惰性的材料(不銹鋼和PEEK)製成的。它很適合水性(FKM和EPDM O形環)和有機溶劑(FFKM O形環)的電解質要求。鍍金針腳可確保良好的電氣接觸。該結構是氣密性的,可以毫不費力地在手套箱中進行組裝,將可能的人為錯誤降到最低。

應用說明
該電池可用於所有常見的電池測量,如恒電流循環、循環伏安法或電化學阻抗頻譜。液體和固態或凝膠聚合物的電解質都可以被研究。此外,還可以研究超級電容器材料的特性和性能。可以檢查各種材料,包括典型的鋰離子電極(石墨、NMC、LTO等)和其它化學材料 ——鈉、鎂、鉀…。它還可以應用於測量隔板和電解質的離子電導率。

規格

  • 推薦電極直徑:18 mm(其他選項:12 mm、15 mm、16 mm)
  • 推薦最小隔板直徑:電極直徑 + 2 mm(最大 22 mm)
  • 最大電極夾層厚度:2.5 mm
  • 工作溫度:-40°C – 70°C 

產品包括

  • 1x帶溫度感測器界面的三電極盒
  • 1x參考電極沖頭
  • 1x上柱塞(不銹鋼316L/317L)
  • 1x下柱塞(不銹鋼316L/317L) 
  • 1x隔板鎖環 
  • 1 x O形環

Select electrolyte type:

  • organic electrolyte
  • water-based electrolyte

Select elelctrode diameter:

  • 18 mm(default)
  • 12 mm
  • 15 mm
  • 16 mm

This is default cartridge included in Three Electrode Battery Test Cell and other redox.me battery test cells. It is ideal choice when researcher wants to perform reproducible electrochemical measurements of battery and supercapacitor materials under controlled compression in a three-electrode setup. The battery cartridges are exchangeable between cell bases, therefore it is convenient to have multiple cartridges and use one while the other is in cleaning etc.

The Battery Cartridge – Three Electrode Setup consists of upper and lower electrode plungers, separator lock ring and reference electrode punch. The (default) electrode plungers are designed for planar electrodes with diameter of 18 mm and total sandwich thickness up to 2.5 mm. The diameter of separator shall be at least 2 mm larger than electrode diameter (max. 22 mm). The lock ring secures the separator in the electrode cartridge allowing easy and safe electrodes insertion, while ensuring accurate alignment. The upper and lower electrode plungers are available in various materials: 316L/317L Stainless Steel (default), copper, aluminum, nickel, gold plated nickel, etc. The punch-type reference electrode is installed from the side of the electrode cartridge. Thanks to sharp edged hole at the end of the pin the reference electrode (Li/Na/K etc.) can be easily punched from the metal foil and directly loaded into cell. The magnetic mount facilitates rapid assembly of the cartridge in the cell base For 2-electrode measurements the reference electrode feedthrough hole can be closed with the reference electrode punch.
The battery cartridge elements are constructed with materials that are inert to the sample (Stainless steel 316L/317L and PEEK). It well fits aqueous (FKM and EPDM O-Rings) and organic solvent (FFKM O-Rings) electrolyte requirements. Good electrical contact is ensured by gold plated pins. The battery cartridge can be effortlessly installed in the Three Electrode Battery Test Cell even when operating in the glove box, reducing possible human error to minimum.

Application note 
This cell can be used for all common battery measurements, such as galvanostatic cycling, cyclic voltammetry or electrochemical impedance spectroscopy. Both liquid and solid-state electrolytes can be studied. Additionally, properties and performance of supercapacitor materials can be investigated. Various materials can be examined, including typical Li-ion electrodes (graphite, NMC, LTO, etc.) and other chemistries – sodium, magnesium, potassium etc. It can also be applied to measure the ionic conductivity of separators and electrolytes.

Specification 

  • default electrode diameter: 18 mm (other options: 12 mm, 15 mm, 16 mm)
  • recommended minimum separator diameter: electrode diameter + 2 mm (max. 22 mm)
  • maximum electrode sandwich thickness: 2.5 mm 
  • operating temperature: -40°C – 80°C

Product includes 

  • 1 x three-electrode cartridge with temperature sensor port
  • 1 x punch-type reference electrode  
  • 1 x upper plunger (Stainless Steel 316L/317L) 
  • 1 x lower plunger (Stainless Steel 316L/317L) 
  • 1 x separator locking ring 
  • 1 x set of O-Rings